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Methods of Separating Mixtures and purifying substances

 

Filtration and Evaporation

Rock salt is a mixture of salt and sand.

Salt and sand are both compounds but because the salt is soluble in water and the sand isn't, the two can be separated using the following methods:

 

Simple Distillation

Simple distillation is used to separate a mixture of a liquid and a solid, for example ink.

(1) The liquid is heated and boils off.

(2) The vapour is cooled by cold water, condensed and collected leaving the solid behind.

This can be used to purify sea water or tap water.

A labeled, detailed 3D scientific diagram illustrating the laboratory apparatus used for distillation, set against a plain light gray studio background. Multiple heavy, metallic square bases support tall metal vertical rods with adjustable clamps holding the glassware. At the top right, an engraved metallic plaque reads "Distillation Apparatus."

On the left side, a gas burner (labeled "Burner") sits on a base, connected by a black gas tube, emitting a light-blue flame. Above the flame, a round-bottom flask (labeled "Distilling Flask") sits on a metallic gauze and triangle support, clamped to the stand. The flask contains a bubbling, light-blue boiling liquid with wisps of vapor (labeled "Vapors") rising. A stopper closes the top of the distilling flask, and a glass thermometer (labeled "Thermometer") with a red internal column is inserted through the stopper.

A horizontal glass connecting tube joins the distilling flask to the top of a long, inclined glass condenser (labeled "Condenser"). This complex glass tube contains an internal spiral (coiled) tube. The outer jacket of the condenser is filled with a light-blue cooling fluid. Two black rubber tubes connect to ports on the condenser jacket, secured by metal hose clamps: the lower tube on the right is labeled "Cold Water In," and the upper tube on the left is labeled "Water Out."

The lower end of the condenser ends in an elbow adapter that drips clear liquid drops (labeled "Distillate") into a glass conical flask (labeled "Receiving Flask") sitting on a separate base to the right. The receiving flask contains a small amount of collected clear liquid. All key components are connected with thin lines leading to clear text labels.

Distillation experiment

 

 

 

Fractional Distillation

Fractional distillation is used for separating a mixture of liquids.

(1) The mixture of liquids are heated and each boil off at their own temperature.

(2) The vapour passes up through a fractionating column.

(3) The vapour is cooled by cold water, condensed and collected.

Fractional distillation is used on a large scale to separate the components of crude oil, because the different hydrocarbons have different boiling points (Distillation of crude oil).

 

 

🧪 Knowledge Check: Separation Techniques

Test your understanding of the different methods used to separate mixtures in the laboratory.

1. Which method would be most suitable for separating sand from a mixture of sand and water?

2. In evaporation, what is left behind in the evaporating dish after the liquid has turned into a gas?

3. Which technique relies on substances having different boiling points to separate them?

4. Chromatography separates substances like ink dyes based on which property?

5. Which technique would you use to separate two liquids that do not mix (immiscible), such as oil and water?

Click to Reveal Answers
1. Filtration (Used for insoluble solids like sand).
2. The solid solute (The liquid evaporates, leaving the solid behind).
3. Distillation (Boiling points determine which liquid evaporates first).
4. Solubility in a solvent (Different dyes travel different distances).
5. Decanting or using a separating funnel (Used for liquids that naturally separate into layers).

 

 

Tags:Filtration, Evaporation, Fractional distillation, Simple distillation

 

 

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